Outputs (1143)

DSC study of sucrose melting (2006)
Journal Article
Beckett, S. T., Francesconi, M. G., Geary, P. M., Mackenzie, G., & Maulny, A. P. (2006). DSC study of sucrose melting. Carbohydrate Research, 341(15), 2591-2599. https://doi.org/10.1016/j.carres.2006.07.004

An early endothermic peak at ∼150 °C was observed for crystalline sucrose by differential scanning calorimetry. The enthalpy at this temperature was found to vary with recrystallised sucrose from different sources. The addition of mineral salts to re... Read More about DSC study of sucrose melting.

Magnetic coupling and long-range order in the spin-chain sulfide Ba 2CoS3 (2006)
Journal Article
Barnes, A. D., Baikie, T., Hardy, V., Lepetit, M. B., Maignan, A., Young, N. A., & Francesconi, M. G. (2006). Magnetic coupling and long-range order in the spin-chain sulfide Ba 2CoS3. Journal of Materials Chemistry, 16(34), 3489-3502. https://doi.org/10.1039/b605178b

In this paper, we report on the magnetic properties of Ba 2CoS3, a spin-chain compound recently found to be the first Co2+-containing one-dimensional sulfide to show metallic-like conductivity and negative magnetoresistance. We carried out an in-dept... Read More about Magnetic coupling and long-range order in the spin-chain sulfide Ba 2CoS3.

Complexes of tungsten(IV,VI) derived from linked aryloxide ligands (2006)
Journal Article
Redshaw, C., & Humphrey, S. M. (2006). Complexes of tungsten(IV,VI) derived from linked aryloxide ligands. Polyhedron, 25(9), 1946-1954. https://doi.org/10.1016/j.poly.2005.12.008

Biphenoxo complexes of tungsten(VI), [WCl4{CHR[C6H2(But)2O]2}] R = H (1), Me (2) are reduced by Na/Hg in the presence of PMe3 to give cis, trans-WCl2(PMe3)2{CHR[C6H2(But)2O]2} R = H (3), Me (4). Reaction of [WOCl4] with the biphenols 2,2′-CHR[C6H2(Bu... Read More about Complexes of tungsten(IV,VI) derived from linked aryloxide ligands.

General method of preparation of mesoporous M/Si3N4 nano-composites via a non-aqueous sol-gel route (2005)
Journal Article
Cheng, F., Kelly, S. M., Young, N. A., Clark, S., Francesconi, M. G., Lefebvre, F., & Bradley, J. S. (2005). General method of preparation of mesoporous M/Si3N4 nano-composites via a non-aqueous sol-gel route. Chemical communications : Chem comm / the Royal Society of Chemistry, 5662-5664. https://doi.org/10.1039/b511790a

We report a general method for the preparation of transition-metal silicon nitride nanocomposites; for example, mesoporous Pd-Si 3 N 4 nanocomposite materials with high surface area were prepared by pyrolysis of a silicon palladium imide-chloride co... Read More about General method of preparation of mesoporous M/Si3N4 nano-composites via a non-aqueous sol-gel route.

Thioglycosylated cationic porphyrins––convenient synthesis and photodynamic activity in vitro (2004)
Journal Article
Ahmed, S., Davoust, E., Savoie, H., Boa, A. N., & Boyle, R. W. (2004). Thioglycosylated cationic porphyrins––convenient synthesis and photodynamic activity in vitro. Tetrahedron letters; the international organ for the rapid publication of preliminary communications in organic chemistry, 45(31), 6045-6047. https://doi.org/10.1016/j.tetlet.2004.06.021

A convenient and flexible synthesis of meso-tetraaryl porphyrins substituted with three thioglycosyl units, and also bearing one pyridyl substituent is reported. Quaternisation of the pyridine nitrogen with alkyl iodides gives access to a range of wa... Read More about Thioglycosylated cationic porphyrins––convenient synthesis and photodynamic activity in vitro.

Ba2−xSrxPdO2F2(0 ≤ x ≤ 1.5): The first palladium-oxide-fluorides (2003)
Journal Article
Baikie, T., Dixon, E. L., Young, N. A., Rooms, J. F., & Francesconi, M. G. (2003). Ba2−xSrxPdO2F2(0 ≤ x ≤ 1.5): The first palladium-oxide-fluorides. Chemical communications : Chem comm / the Royal Society of Chemistry, 3(13), 1580-1581. https://doi.org/10.1039/b303402j

The first series of alkaline-earth palladium oxide-fluorides Ba2−xSrxPdO2F2(0 ≤ x ≤ 1.5) display the T′ structure (Nd2CuO4) instead of the predicted T structure (La2CuO4), showing that electronic factors prevail over steric factors.

Selectivity and enantioselectivity in the palladium catalysed hydrogenation of pyrazine and some substituted pyrazines (2000)
Thesis
Carroll, J. R. (2000). Selectivity and enantioselectivity in the palladium catalysed hydrogenation of pyrazine and some substituted pyrazines. (Thesis). University of Hull. Retrieved from https://hull-repository.worktribe.com/output/4240018

The palladium catalysed hydrogenation of pyrazine and some substituted pyrazines has been investigated over a range of reaction conditions.
This thesis reports and discusses work in three areas. The first being the hydrogenation of pyrazine over Pd/... Read More about Selectivity and enantioselectivity in the palladium catalysed hydrogenation of pyrazine and some substituted pyrazines.

A versatile family of interconvertible microporous chiral molecular frameworks: The first example of ligand control of network chirality (2000)
Journal Article
Kepert, C. J., Prior, T. J., & Rosseinsky, M. J. (2000). A versatile family of interconvertible microporous chiral molecular frameworks: The first example of ligand control of network chirality. Journal of the American Chemical Society, 122(21), 5158-5168. https://doi.org/10.1021/ja993814s

Two families of molecular frameworks which grow as homochiral single crystals are described. Both consist of multiple interpenetration of the three-connected chiral (10,3)-a (Y*) network and result from the tridentate coordination of the 1,3,5-benzen... Read More about A versatile family of interconvertible microporous chiral molecular frameworks: The first example of ligand control of network chirality.

Antiferroelectric liquid crystals : hosts and binary mixtures (2000)
Thesis
Parghi, D. D. (2000). Antiferroelectric liquid crystals : hosts and binary mixtures. (Thesis). University of Hull. Retrieved from https://hull-repository.worktribe.com/output/4408280

This thesis details the work carried out towards a doctoral degree in the synthesis, characterisation and evaluation of liquid-crystalline materials possessing antiferroelectric smectic C* (SmCA*) and non-chiral anticlinic smectic C (SmCait) phases.... Read More about Antiferroelectric liquid crystals : hosts and binary mixtures.

Who is in control? An investigation of nurse and patient beliefs relating to control of their health care (1994)
Journal Article
Smith, R., & Draper, P. (1994). Who is in control? An investigation of nurse and patient beliefs relating to control of their health care. Journal of advanced nursing, 19(5), 884-892. https://doi.org/10.1111/j.1365-2648.1994.tb01165.x

This study compares nurse and patient beliefs regarding control of health and perceptions of the amount of patient control. Data were collected from 21 nurses and 32 patients on a mixed surgical ward, using a series of self‐report questionnaires. No... Read More about Who is in control? An investigation of nurse and patient beliefs relating to control of their health care.