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Operando study of the dynamic evolution of multiple Fe-rich intermetallics of an Al recycled alloy in solidification by synchrotron X-ray and machine learning (2024)
Journal Article
Xiang, K., Qin, L., Zhao, Y., Huang, S., Du, W., Boller, E., Rack, A., Li, M., & Mi, J. (2024). Operando study of the dynamic evolution of multiple Fe-rich intermetallics of an Al recycled alloy in solidification by synchrotron X-ray and machine learning. Acta Materialia, 279, Article 120267. https://doi.org/10.1016/j.actamat.2024.120267

Using synchrotron X-ray diffraction, tomography and machine-learning enabled phase segmentation strategy, we have studied under operando conditions the nucleation, co-growth and dynamic interplays among the dendritic and multiple intermetallic phases... Read More about Operando study of the dynamic evolution of multiple Fe-rich intermetallics of an Al recycled alloy in solidification by synchrotron X-ray and machine learning.

Synchrotron X-ray operando study and multiphysics modelling of the solidification dynamics of intermetallic phases under electromagnetic pulses (2023)
Journal Article
Qin, L., Du, W., Cipiccia, S., Bodey, A. J., Rau, C., & Mi, J. (2024). Synchrotron X-ray operando study and multiphysics modelling of the solidification dynamics of intermetallic phases under electromagnetic pulses. Acta Materialia, 265, Article 119593. https://doi.org/10.1016/j.actamat.2023.119593

In this paper, we used synchrotron X-ray radiography and tomography to study systematically and in operando conditions the growth dynamics of the primary Al3Ni intermetallic phases in an Al-15wt%Ni alloy in the solidification process with magnetic pu... Read More about Synchrotron X-ray operando study and multiphysics modelling of the solidification dynamics of intermetallic phases under electromagnetic pulses.

3D phase field modeling of multi-dendrites evolution in solidification and validation by synchrotron x-ray tomography (2021)
Journal Article
Wang, S., Guo, Z., Kang, J., Zou, M., Li, X., Zhang, A., Du, W., Zhang, W., Lee, T. L., Xiong, S., & Mi, J. (2021). 3D phase field modeling of multi-dendrites evolution in solidification and validation by synchrotron x-ray tomography. Materials, 14(3), Article 520. https://doi.org/10.3390/ma14030520

© 2021 by the authors. Licensee MDPI, Basel, Switzerland. In this paper, the dynamics of multi-dendrite concurrent growth and coarsening of an Al-15 wt.% Cu alloy was studied using a highly computationally efficient 3D phase field model and real-time... Read More about 3D phase field modeling of multi-dendrites evolution in solidification and validation by synchrotron x-ray tomography.

Multiscale characterization of the nucleation and 3D structure of Al3Sc phases using electron microscopy and synchrotron X-ray tomography (2020)
Journal Article
Zhao, Y., Zhang, W., Koe, B., Du, W., Wang, M., Wang, W., Boller, E., Rack, A., Sun, Z., Shu, D., Sun, B., & Mi, J. (2020). Multiscale characterization of the nucleation and 3D structure of Al3Sc phases using electron microscopy and synchrotron X-ray tomography. Materials Characterization, 164, Article 110353. https://doi.org/10.1016/j.matchar.2020.110353

Scandium (Sc) has been long recognized as one of the most effective grain refining elements for Al alloys because of the Al3Sc phases formed in an Al melt containing Sc. However, there are still lack of comprehensive studies on the exact mechanism of... Read More about Multiscale characterization of the nucleation and 3D structure of Al3Sc phases using electron microscopy and synchrotron X-ray tomography.

In-situ synchrotron X-ray imaging and tomography studies of the evolution of solidification microstructures under pulse electromagnetic fields (2018)
Thesis
Du, W. (2018). In-situ synchrotron X-ray imaging and tomography studies of the evolution of solidification microstructures under pulse electromagnetic fields. (Thesis). University of Hull. Retrieved from https://hull-repository.worktribe.com/output/4221948

This research studies the dynamic evolution of dendritic structures and intermetallic phases of four Al based alloys during the solidification under pulse electromagnetic fields (PMFs). An advanced PMF solidification device was upgraded, built, commi... Read More about In-situ synchrotron X-ray imaging and tomography studies of the evolution of solidification microstructures under pulse electromagnetic fields.

3D characterisation of the Fe-rich intermetallic phases in recycled Al alloys by synchrotron X-ray microtomography and skeletonisation (2018)
Journal Article
Schlepütz, C. M., Zhao, Y., Du, W., Koe, B., Connolley, T., Irvine, S., Allan, P. K., Schlepütz, C. M., Zhang, W., Wang, F., Eskin, D. G., & Mi, J. (2018). 3D characterisation of the Fe-rich intermetallic phases in recycled Al alloys by synchrotron X-ray microtomography and skeletonisation. Scripta materialia, 146, 321-326. https://doi.org/10.1016/j.scriptamat.2017.12.010

© 2017 Elsevier Ltd Synchrotron X-ray microtomography and skeletonisation method were used to study the true 3D network structures and morphologies of the Fe-rich intermetallic phases in recycled Al-5.0%Cu-0.6%Mn alloys with 0.5% and 1.0% Fe. It was... Read More about 3D characterisation of the Fe-rich intermetallic phases in recycled Al alloys by synchrotron X-ray microtomography and skeletonisation.