Sharif Hussein Sharif Zein
Synthesis and characterization of TiO2 coated multiwalled carbon nanotubes using a sol gel method
Sharif Zein, Sharif Hussein; Boccaccini, Aldo R.
Authors
Aldo R. Boccaccini
Abstract
A considerable improvement in the quality of TiO 2 coatings on multiwalled carbon nanotubes (MWNTs) was obtained by introducing a three-step purification and functionalization process which combines oxidation in air followed by sulfuric acid refluxes and reoxidation in air before synmesis of the TiO 2 coating by the sol-gel method. A range of techniques, including transmission electron microscopy (TEM), scanning electron microscopy (SEM), energy dispersive X-rays (EDX), X-ray diffraction (XRD), Raman spectroscopy, and thermal gravimetric analysis (TGA) were applied to characterize TiO 2 coated MWNTs obtained by sol-gel. TEM results showed that the MWNTs were fully and homogeneously coated wim TiO 2 while SEM coupled with EDX confirmed me presence of a thick layer of TiO 2 coating the MWNTs. XRD and Raman spectroscopy results revealed that the crystalline structure of TiO 2 on the surface of MWNTs was anatase.
Citation
Sharif Zein, S. H., & Boccaccini, A. R. (2008). Synthesis and characterization of TiO2 coated multiwalled carbon nanotubes using a sol gel method. Industrial & engineering chemistry research, 47(17), 6598-6606. https://doi.org/10.1021/ie701770q
Journal Article Type | Article |
---|---|
Online Publication Date | Jul 30, 2008 |
Publication Date | Sep 3, 2008 |
Deposit Date | Nov 13, 2014 |
Journal | Industrial & Engineering Chemistry Research |
Print ISSN | 0888-5885 |
Publisher | American Chemical Society |
Peer Reviewed | Peer Reviewed |
Volume | 47 |
Issue | 17 |
Pages | 6598-6606 |
DOI | https://doi.org/10.1021/ie701770q |
Keywords | Industrial and Manufacturing Engineering; General Chemistry; General Chemical Engineering |
Public URL | https://hull-repository.worktribe.com/output/368800 |
Contract Date | Nov 13, 2014 |
You might also like
Downloadable Citations
About Repository@Hull
Administrator e-mail: repository@hull.ac.uk
This application uses the following open-source libraries:
SheetJS Community Edition
Apache License Version 2.0 (http://www.apache.org/licenses/)
PDF.js
Apache License Version 2.0 (http://www.apache.org/licenses/)
Font Awesome
SIL OFL 1.1 (http://scripts.sil.org/OFL)
MIT License (http://opensource.org/licenses/mit-license.html)
CC BY 3.0 ( http://creativecommons.org/licenses/by/3.0/)
Powered by Worktribe © 2024
Advanced Search