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3D local atomic structure evolution in a solidifying Al-0.4Sc dilute alloy melt revealed in operando by synchrotron X-ray total scattering and modelling (2022)
Journal Article
Huang, S., Luo, S., Qin, L., Shu, D., Sun, B., Lunt, A. J. G., Korsunsky, A. M., & Mi, J. (2022). 3D local atomic structure evolution in a solidifying Al-0.4Sc dilute alloy melt revealed in operando by synchrotron X-ray total scattering and modelling. Scripta materialia, 211, Article 114484. https://doi.org/10.1016/j.scriptamat.2021.114484

Using synchrotron X-ray total scattering and empirical potential structure refinement modelling, we studied systematically in operando condition the disorder-to-order local atomic structure transition in a pure Al and a dilute Al-0.4Sc alloy melt in... Read More about 3D local atomic structure evolution in a solidifying Al-0.4Sc dilute alloy melt revealed in operando by synchrotron X-ray total scattering and modelling.

Ultrafast synchrotron X-ray imaging and multiphysics modelling of liquid phase fatigue exfoliation of graphite under ultrasound (2021)
Journal Article
Qin, L., Maciejewska, B. M., Subroto, T., Morton, J. A., Porfyrakis, K., Tzanakis, I., Eskin, D. G., Grobert, N., Fezzaa, K., & Mi, J. (2022). Ultrafast synchrotron X-ray imaging and multiphysics modelling of liquid phase fatigue exfoliation of graphite under ultrasound. Carbon, 186, 227-237. https://doi.org/10.1016/j.carbon.2021.10.014

Ultrasound-assisted liquid phase exfoliation is a promising method for manufacturing of 2D materials in large scale and sustainable manner. A large number of studies using ex-situ nano/micro structural characterization techniques have been made to in... Read More about Ultrafast synchrotron X-ray imaging and multiphysics modelling of liquid phase fatigue exfoliation of graphite under ultrasound.

Characterization of the Convoluted 3D Intermetallic Phases in a Recycled Al Alloy by Synchrotron X-ray Tomography and Machine Learning (2021)
Journal Article
Li, Z., Qin, L., Guo, B., Yuan, J., Zhang, Z., Li, W., & Mi, J. (2022). Characterization of the Convoluted 3D Intermetallic Phases in a Recycled Al Alloy by Synchrotron X-ray Tomography and Machine Learning. Acta Metallurgica Sinica (English Letters), 35(1), 115–123. https://doi.org/10.1007/s40195-021-01312-3

Fe-rich intermetallic phases in recycled Al alloys often exhibit complex and 3D convoluted structures and morphologies. They are the common detrimental intermetallic phases to the mechanical properties of recycled Al alloys. In this study, we used sy... Read More about Characterization of the Convoluted 3D Intermetallic Phases in a Recycled Al Alloy by Synchrotron X-ray Tomography and Machine Learning.

Synchrotron X-ray imaging and ultrafast tomography in situ study of the fragmentation and growth dynamics of dendritic microstructures in solidification under ultrasound (2021)
Journal Article
Zhang, Z., Wang, C., Koe, B., Schlepütz, C. M., Irvine, S., & Mi, J. (2021). Synchrotron X-ray imaging and ultrafast tomography in situ study of the fragmentation and growth dynamics of dendritic microstructures in solidification under ultrasound. Acta Materialia, 209, Article 116796. https://doi.org/10.1016/j.actamat.2021.116796

High speed synchrotron X-ray imaging and ultrafast tomography were used to study in situ and in real time the fragmentation and growth dynamics of dendritic microstructures of an Al-15%Cu alloy in solidification under ultrasound. An ultrasound of 30... Read More about Synchrotron X-ray imaging and ultrafast tomography in situ study of the fragmentation and growth dynamics of dendritic microstructures in solidification under ultrasound.

Multiscale characterization of the 3D network structure of metal carbides in a Ni superalloy by synchrotron X-ray microtomography and ptychography (2020)
Journal Article
Zhang, Z., Khong, J. C., Koe, B., Luo, S., Huang, S., Qin, L., Cipiccia, S., Batey, D., Bodey, A. J., Rau, C., Chiu, Y. L., Zhang, Z., Gebelin, J. C., Green, N., & Mi, J. (2021). Multiscale characterization of the 3D network structure of metal carbides in a Ni superalloy by synchrotron X-ray microtomography and ptychography. Scripta materialia, 193, 71-76. https://doi.org/10.1016/j.scriptamat.2020.10.032

Synchrotron X-ray microtomography and ptychography were used to characterize the 3D network structure, morphology and distribution of metal carbides in an as-cast IN713LC Ni superalloy. MC typed carbides were found to distribute mainly on the grain b... Read More about Multiscale characterization of the 3D network structure of metal carbides in a Ni superalloy by synchrotron X-ray microtomography and ptychography.

A novel electromagnetic apparatus for in-situ synchrotron X-ray imaging study of the separation of phases in metal solidification (2020)
Journal Article
Koe, B., Abraham, C., Bailey, C., Greening, B., Small, M., Connolley, T., & Mi, J. (2020). A novel electromagnetic apparatus for in-situ synchrotron X-ray imaging study of the separation of phases in metal solidification. HardwareX, 7, Article e00104. https://doi.org/10.1016/j.ohx.2020.e00104

As a part of a research into new techniques for purifying recycled aluminium alloys, a novel electromagnetic apparatus had been developed for investigating in real-time the separation mechanisms of detrimental inclusions in aluminium alloy melts unde... Read More about A novel electromagnetic apparatus for in-situ synchrotron X-ray imaging study of the separation of phases in metal solidification.

Modelling and neutron diffraction characterization of the interfacial bonding of spray formed dissimilar steels (2018)
Journal Article
Lee, T. L., Mi, J., Ren, S., Zhao, S., Fan, J., Kabra, S., Zhang, S., & Grant, P. S. (2018). Modelling and neutron diffraction characterization of the interfacial bonding of spray formed dissimilar steels. Acta Materialia, 155, 318-330. https://doi.org/10.1016/j.actamat.2018.05.055

The spray forming of thick, dissimilar steel clad tubes with the objective of achieving a high integrity metallurgical bond across the cladding-substrate interface able to withstand residual stresses and subsequent thermo-mechanical processing was in... Read More about Modelling and neutron diffraction characterization of the interfacial bonding of spray formed dissimilar steels.

3D characterisation of the Fe-rich intermetallic phases in recycled Al alloys by synchrotron X-ray microtomography and skeletonisation (2018)
Journal Article
Schlepütz, C. M., Zhao, Y., Du, W., Koe, B., Connolley, T., Irvine, S., Allan, P. K., Schlepütz, C. M., Zhang, W., Wang, F., Eskin, D. G., & Mi, J. (2018). 3D characterisation of the Fe-rich intermetallic phases in recycled Al alloys by synchrotron X-ray microtomography and skeletonisation. Scripta materialia, 146, 321-326. https://doi.org/10.1016/j.scriptamat.2017.12.010

© 2017 Elsevier Ltd Synchrotron X-ray microtomography and skeletonisation method were used to study the true 3D network structures and morphologies of the Fe-rich intermetallic phases in recycled Al-5.0%Cu-0.6%Mn alloys with 0.5% and 1.0% Fe. It was... Read More about 3D characterisation of the Fe-rich intermetallic phases in recycled Al alloys by synchrotron X-ray microtomography and skeletonisation.

Ultrafast synchrotron X-ray imaging studies of microstructure fragmentation in solidification under ultrasound (2017)
Journal Article
Wang, B., Tan, D., Lee, T. L., Khong, J. C., Wang, F., Eskin, D., Connolley, T., Fezzaa, K., & Mi, J. (2018). Ultrafast synchrotron X-ray imaging studies of microstructure fragmentation in solidification under ultrasound. Acta Materialia, 144, 505-515. https://doi.org/10.1016/j.actamat.2017.10.067

Ultrasound processing of metal alloys is an environmental friendly and promising green technology for liquid metal degassing and microstructural refinement. However many fundamental issues in this field are still not fully understood, because of the... Read More about Ultrafast synchrotron X-ray imaging studies of microstructure fragmentation in solidification under ultrasound.