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Silicon diimide gel as an efficient stationary phase in thin layer chromatography for acid-sensitive organic compounds

Kitney, Stuart P.; Sajedin, Seyed M.; Rocher, Vincent; Cheng, Fei; Kelly, Stephen M.

Authors

Stuart P. Kitney

Seyed M. Sajedin

Vincent Rocher

Fei Cheng



Abstract

We report the use of mesoporous silicon diimide gel as a basic stationary phase in thin layer chromatography for the characterisation and purification of acid-sensitive compounds. The gel is prepared by a simple sol-gel process and exhibits a large specific surface area, almost monodisperse pores and basic properties due to free-hanging amine groups.

Citation

Kitney, S. P., Sajedin, S. M., Rocher, V., Cheng, F., & Kelly, S. M. (2017). Silicon diimide gel as an efficient stationary phase in thin layer chromatography for acid-sensitive organic compounds. Chemical communications : Chem comm / the Royal Society of Chemistry, 53(80), 11080-11082. https://doi.org/10.1039/c7cc04952h

Journal Article Type Article
Acceptance Date Sep 19, 2017
Online Publication Date Sep 19, 2017
Publication Date Sep 19, 2017
Deposit Date Sep 21, 2017
Publicly Available Date Sep 19, 2018
Journal Chemical communications
Print ISSN 1359-7345
Electronic ISSN 1364-548X
Publisher Royal Society of Chemistry
Peer Reviewed Peer Reviewed
Volume 53
Issue 80
Pages 11080-11082
DOI https://doi.org/10.1039/c7cc04952h
Keywords Silicon diimide gel; Thin layer chromatography; Basic stationary phase
Public URL https://hull-repository.worktribe.com/output/454896
Publisher URL http://pubs.rsc.org/en/Content/ArticleLanding/2017/CC/C7CC04952H#!divAbstract
Additional Information : This document is CrossCheck deposited; : Stuart P. Kitney (ORCID); : Stephen M. Kelly (ORCID); : The Royal Society of Chemistry has an exclusive publication licence for this journal; : Received 26 June 2017; Accepted 19 September 2017; Accepted Manuscript published 19 September 2017; Advance Article published 26 September 2017; Version of Record published 5 October 2017

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