Improved DNA extraction efficiency from low level cell numbers using a silica monolith based micro fluidic device

Kashkary, Loay; Kemp, Cordula; Shaw, Kirsty J.; Greenway, Gillian M.; Haswell, Stephen J.

doi:10.1016/j.aca.2012.05.019

Synthesis, characterization, and the ethylene (co-)polymerization behaviour of half-titanocene dichloride 2-aryliminoquinolin-8-olates (2012)
Journal Article
Huang, W., Zhang, W., Sun, W. H., Wang, L., & Redshaw, C. (2012). Synthesis, characterization, and the ethylene (co-)polymerization behaviour of half-titanocene dichloride 2-aryliminoquinolin-8-olates. Catalysis science & technology, 12(10), 2090-2098. https://doi.org/10.1039/c2cy20240a

A series of half-titanocene dichloride 2-aryliminoquinolin-8-olates, CpTi LCl2 (C1-C6: Cp as C5H5, L as 2-(1-(o-benzhydrylarylimino)methyl)quinolin-8-olates or 2-(1-(o- benzhydrylarylimino)ethyl)quinolin-8-olates), was synthesized and fully character... Read More about Synthesis, characterization, and the ethylene (co-)polymerization behaviour of half-titanocene dichloride 2-aryliminoquinolin-8-olates.

Mental capacity and working memory in chemistry: Algorithmic versus open-ended problem solving (2012)
Journal Article
Clair-Thompson, H. S., Overton, T., & Bugler, M. (2012). Mental capacity and working memory in chemistry: Algorithmic versus open-ended problem solving. Chemistry Education Research and Practice, 13(4), 484-489. https://doi.org/10.1039/c2rp20084h

Previous research has revealed that problem solving and attainment in chemistry are constrained by mental capacity and working memory. However, the terms mental capacity and working memory come from different theories of cognitive resources, and are... Read More about Mental capacity and working memory in chemistry: Algorithmic versus open-ended problem solving.

Synthesis, structure and fluorescent properties of 2-(1H-benzoimidazol-2- yl)quinolin-8-ol ligands and their zinc complexes (2012)
Journal Article
Xia, J., Zhou, Z., Li, W., Zhang, H. Q., Redshaw, C., & Sun, W. H. (2013). Synthesis, structure and fluorescent properties of 2-(1H-benzoimidazol-2- yl)quinolin-8-ol ligands and their zinc complexes. Inorganica Chimica Acta, 394, 569-575. https://doi.org/10.1016/j.ica.2012.09.012

A series of 2-(1H-benzoimidazol-2-yl)quinolin-8-ol ligands (L1-L5) and their Zn(II) complexes (C1-C6) were synthesized and characterized by spectroscopic and elemental analyses. The molecular structures of C1 and C6 were confirmed by single-crystal X... Read More about Synthesis, structure and fluorescent properties of 2-(1H-benzoimidazol-2- yl)quinolin-8-ol ligands and their zinc complexes.

Trimetallic yttrium N-(2-methylquinolin-8-yl)benzamides: Synthesis, structure and use in ring-opening polymerization (ROP) of ε-caprolactone (2012)
Journal Article
Zhang, W., Liu, S., Sun, W. H., Hao, X., & Redshaw, C. (2012). Trimetallic yttrium N-(2-methylquinolin-8-yl)benzamides: Synthesis, structure and use in ring-opening polymerization (ROP) of ε-caprolactone. New journal of chemistry = Nouveau journal de chimie, 36(11), 2392-2396. https://doi.org/10.1039/c2nj40711f

A series of trimetallic yttrium complexes, L7Y 3Cl2 [L = N-(2-methylquinolin-8-yl)-p-R-benzamides, 1: R = H; 2: R = OMe; 3: R = Me; 4: R = Cl], has been synthesized by the stoichiometric reaction of YCl3(THF)2 with the corresponding potassium amidate... Read More about Trimetallic yttrium N-(2-methylquinolin-8-yl)benzamides: Synthesis, structure and use in ring-opening polymerization (ROP) of ε-caprolactone.

Synthesis and inclusion properties of C3-symmetric triazole derivatives based on hexahomotrioxacalix[3]arene (2012)
Journal Article
Jin, C. C., Kinoshita, T., Cong, H., Ni, X. L., Zeng, X., Hughes, D. L., Redshaw, C., & Yamato, T. (2012). Synthesis and inclusion properties of C3-symmetric triazole derivatives based on hexahomotrioxacalix[3]arene. New journal of chemistry = Nouveau journal de chimie, 36(12), 2580-2586. https://doi.org/10.1039/c2nj40599g

A series of metal ion receptors cone-7,15,23-tri-tert-butyl-25,26,27- tris{[1H-(1-arylmethyl)(1,2,3-triazolyl)]-4-methoxy}hexahomotrioxacalix[3] arenes, cone-3-cone-5, have been synthesized from 7,15,23-tri-tert-butyl-25,26, 27-tris(propargyloxy)hexa... Read More about Synthesis and inclusion properties of C3-symmetric triazole derivatives based on hexahomotrioxacalix[3]arene.

2-(1-(Arylimino)ethyl)-8-arylimino-5,6,7-trihydroquinolylcobalt dichloride: Synthesis and polyethylene wax formation (2012)
Journal Article
Sun, W. H., Kong, S., Chai, W., Shiono, T., Redshaw, C., Hu, X., Guo, C., & Hao, X. (2012). 2-(1-(Arylimino)ethyl)-8-arylimino-5,6,7-trihydroquinolylcobalt dichloride: Synthesis and polyethylene wax formation. Applied catalysis. A, General, 447-448, 67-73. https://doi.org/10.1016/j.apcata.2012.09.011

A series of 2-(1-(arylimino)ethyl)-8-arylimino-5,6,7-trihydroquinolylcobalt dichloride (aryl = 2,6-R1-4-R2C6H2) pre-catalysts were synthesized and structurally characterized by FT-IR and elemental analyses. The molecular structures of Co1 (R1 = Me, R... Read More about 2-(1-(Arylimino)ethyl)-8-arylimino-5,6,7-trihydroquinolylcobalt dichloride: Synthesis and polyethylene wax formation.

Vanadium(III) phenoxyimine complexes for ethylene or ε-caprolactone polymerization: Mononuclear versus binuclear pre-catalysts (2012)
Journal Article
Clowes, L., Walton, M., Redshaw, C., Chao, Y., Walton, A., Elo, P., Sumerin, V., & Hughes, D. L. (2013). Vanadium(III) phenoxyimine complexes for ethylene or ε-caprolactone polymerization: Mononuclear versus binuclear pre-catalysts. Catalysis science & technology, 3(1), 152-160. https://doi.org/10.1039/c2cy20571h

The mononuclear {[C6H4NCH(ArO)]2VCl(THF)} (Ar = 2,4-t-Bu2C6H2 (1), Ar = C 6H4 (2)), {O[C6H4NCH(ArO)] 2}VCl(THF) (Ar = 2,4-t-Bu2C6H2 (3), Ar = C6H4 (4)) and the binuclear vanadium(iii) complexes {[C6H4NCH(ArO)]VCl2(THF)2} 2(μ-CH2CH2) (Ar = 2,4-t-Bu2C... Read More about Vanadium(III) phenoxyimine complexes for ethylene or ε-caprolactone polymerization: Mononuclear versus binuclear pre-catalysts.

Dimethylaluminium aldiminophenolates: Synthesis, characterization and ring-opening polymerization behavior towards lactides (2012)
Journal Article
Zhang, W., Wang, Y., Sun, W. H., Wang, L., & Redshaw, C. (2012). Dimethylaluminium aldiminophenolates: Synthesis, characterization and ring-opening polymerization behavior towards lactides. Dalton Transactions : an international journal of inorganic chemistry, 41, 11587-11596. https://doi.org/10.1039/c2dt31215h

The stoichiometric reaction of the salicylaldimine derivatives (L1-L12) with trimethylaluminium afforded the corresponding dimethylaluminium aldiminophenolates (C1-C12), which were fully characterized by NMR spectroscopy and elemental analysis. The m... Read More about Dimethylaluminium aldiminophenolates: Synthesis, characterization and ring-opening polymerization behavior towards lactides.

CPMV-DOX delivers (2012)
Journal Article
Aljabali, A. A. A., Shukla, S., Lomonossoff, G. P., Steinmetz, N. F., & Evans, D. J. (2013). CPMV-DOX delivers. Molecular pharmaceutics, 10(1), 3-10. https://doi.org/10.1021/mp3002057

The plant virus, Cowpea mosaic virus (CPMV), is developed as a carrier of the chemotherapeutic drug doxorubicin (DOX). CPMV-DOX conjugate, in which eighty DOX molecules are covalently bound to external surface carboxylates of the viral nanoparticle (... Read More about CPMV-DOX delivers.

Liquid viruses by nanoscale engineering of capsid surfaces (2012)
Journal Article
Patil, A. J., McGrath, N., Elaine Barclay, J., Evans, D. J., Cölfen, H., Manners, I., Perriman, A. W., & Mann, S. (2012). Liquid viruses by nanoscale engineering of capsid surfaces. Advanced materials, 24(33), 4557-4563. https://doi.org/10.1002/adma.201201032

Surface engineering of plant virus capsids via cationization and stoichiometric coupling of a polymer surfactant coronal layer produces a highly concentrated, solvent-free liquid virus at 28 °C. These ionic bionanoconstructs are viscoelastic, retain... Read More about Liquid viruses by nanoscale engineering of capsid surfaces.

CXCR4 chemokine receptor antagonists: nickel(II) complexes of configurationally restricted macrocycles (2012)
Journal Article
Smith, R., Huskens, D., Daelemans, D., Mewis, R. E., Garcia, C. D., Cain, A. N., Freeman, T. N. C., Pannecouque, C., Clercq, E. D., Schols, D., Hubin, T. J., & Archibald, S. J. (2012). CXCR4 chemokine receptor antagonists: nickel(II) complexes of configurationally restricted macrocycles. Dalton Transactions : an international journal of inorganic chemistry, 41(37), 11369-11377. https://doi.org/10.1039/c2dt31137b

Tetraazamacrocyclic complexes of transition metals provide useful units for incorporating multiple coordination interactions into a single protein binding molecule. They can be designed with available sites for protein interactions via donor atom-con... Read More about CXCR4 chemokine receptor antagonists: nickel(II) complexes of configurationally restricted macrocycles.

2-(1-(Arylimino)ethyl)-8-arylimino-5,6,7-trihydroquinoline iron(II) chloride complexes: synthesis, characterization, and ethylene polymerization behavior (2012)
Journal Article
Zhang, W., Chai, W., Sun, W. H., Hu, X., Redshaw, C., & Hao, X. (2012). 2-(1-(Arylimino)ethyl)-8-arylimino-5,6,7-trihydroquinoline iron(II) chloride complexes: synthesis, characterization, and ethylene polymerization behavior. Organometallics, 31(14), 5039-5048. https://doi.org/10.1021/om300388m

The series of 2-(1-(arylimino)ethyl)-8-arylimino-5,6,7-trihydroquinolines was synthesized and fully characterized, for which data indicated two isomer forms of each due to the migration of a double bond. The corresponding iron dichloride complexes we... Read More about 2-(1-(Arylimino)ethyl)-8-arylimino-5,6,7-trihydroquinoline iron(II) chloride complexes: synthesis, characterization, and ethylene polymerization behavior.

Highly active 8-benzoxazolyl- or 8-benzothiazolyl-2- alkylquinolinylnickel(II) complexes for ethylene dimerization and vinyl polymerization of norbornene (2012)
Journal Article
Hao, P., Song, S., Xiao, T., Li, Y., Redshaw, C., & Sun, W. H. (2013). Highly active 8-benzoxazolyl- or 8-benzothiazolyl-2- alkylquinolinylnickel(II) complexes for ethylene dimerization and vinyl polymerization of norbornene. Polyhedron, 52, 1138-1144. https://doi.org/10.1016/j.poly.2012.06.056

The series of nickel halide complexes LNiX2 (C1-C6, X = Cl; C7-C12, X = Br), where L represents one of 8-benzoxazolyl-2-alkylquinoline or 8-benzothiazolyl-2-alkylquinoline derivatives, have been prepared. The molecular structures of the representativ... Read More about Highly active 8-benzoxazolyl- or 8-benzothiazolyl-2- alkylquinolinylnickel(II) complexes for ethylene dimerization and vinyl polymerization of norbornene.

Enhancing the activity and thermal stability of iron precatalysts using 2-(1-{2,6-bis[bis(4-fluorophenyl)methyl]-4-methylphenylimino}ethyl) -6-[1-(arylimino)ethyl]pyridines (2012)
Journal Article
Sun, W. H., Zhao, W., Yu, J., Zhang, W., Hao, X., & Redshaw, C. (2012). Enhancing the activity and thermal stability of iron precatalysts using 2-(1-{2,6-bis[bis(4-fluorophenyl)methyl]-4-methylphenylimino}ethyl) -6-[1-(arylimino)ethyl]pyridines. Macromolecular Chemistry and Physics, 213(12), 1266-1273. https://doi.org/10.1002/macp.201200051

A series of 2-(1-{2,6-bis[bis(4-fluorophenyl)methyl]-4-methylphenylimino} ethyl)-6- [1-(arylimino)ethyl]pyridine ligands is synthesized and fully characterized. The corresponding iron complexes are prepared and characterized by single-crystal X-ray d... Read More about Enhancing the activity and thermal stability of iron precatalysts using 2-(1-{2,6-bis[bis(4-fluorophenyl)methyl]-4-methylphenylimino}ethyl) -6-[1-(arylimino)ethyl]pyridines.

2-Aldiminophenoxytitanium chloride complexes: Synthesis, characterization, and ethylene (co-)polymerization behavior (2012)
Journal Article
Zhang, W., Wang, Y., Redshaw, C., Hao, X., & Sun, W. H. (2012). 2-Aldiminophenoxytitanium chloride complexes: Synthesis, characterization, and ethylene (co-)polymerization behavior. Journal of organometallic chemistry, 715, 119-128. https://doi.org/10.1016/j.jorganchem.2012.05.048

A series of trichlorotitanium 2-aldiminophenoxylate complexes (C1-C6) was synthesized by the stoichiometric reaction of TiCl 4(THF) 2 with the potassium salts of 6-alkyl-2-aldiminophenolates derived from ligands (L1-L6) bearing a bulky benzhydryl sub... Read More about 2-Aldiminophenoxytitanium chloride complexes: Synthesis, characterization, and ethylene (co-)polymerization behavior.

Pharmacological comparison of novel synthetic fenamate analogues with econazole and 2-APB on the inhibition of TRPM2 channels (2012)
Journal Article
Chen, G.-L., Zeng, B., Eastmond, S., Elsenussi, S. E., Boa, A. N., & Xu, S.-Z. (2012). Pharmacological comparison of novel synthetic fenamate analogues with econazole and 2-APB on the inhibition of TRPM2 channels. British Journal of Pharmacology, 167(6), 1232-1243. https://doi.org/10.1111/j.1476-5381.2012.02058.x

BACKGROUND: Fenamate analogues, econazole and 2-APB are inhibitors of TRPM2 channels, which have been used as research tools. However, these compounds have different chemical structures and therapeutic applications. Here we aimed to investigate the p... Read More about Pharmacological comparison of novel synthetic fenamate analogues with econazole and 2-APB on the inhibition of TRPM2 channels.

2-[1-(2,6-dibenzhydryl-4-chlorophenylimino)ethyl]-6-[1-aryliminoethyl] pyridyl cobalt dichlorides: Synthesis, characterization and ethylene polymerization behavior (2012)
Journal Article
He, F., Zhao, W., Cao, X. P., Liang, T., Redshaw, C., & Sun, W. H. (2012). 2-[1-(2,6-dibenzhydryl-4-chlorophenylimino)ethyl]-6-[1-aryliminoethyl] pyridyl cobalt dichlorides: Synthesis, characterization and ethylene polymerization behavior. Journal of organometallic chemistry, 713, 209-216. https://doi.org/10.1016/j.jorganchem.2012.05.020

A series of 2-[1-(2,6-dibenzhydryl-4-chlorophenylimino)ethyl]-6-[1- aryliminoethyl]pyridyl cobalt(II) dichloride complexes (Co1-Co5) were prepared and characterized by elemental and spectroscopic analysis. The molecular structures of the representati... Read More about 2-[1-(2,6-dibenzhydryl-4-chlorophenylimino)ethyl]-6-[1-aryliminoethyl] pyridyl cobalt dichlorides: Synthesis, characterization and ethylene polymerization behavior.

From existing in situ, high-resolution measurement technologies to lab-on-a-chip – the future of water quality monitoring? (2012)
Journal Article
Wade, A. J., Palmer-Felgate, E. J., Halliday, S. J., Skeffington, R. A., Loewenthal, M., Jarvie, H. P., Bowes, M. J., Greenway, G. M., Haswell, S. J., Bell, I. M., Joly, E., Fallatah, A., Neal, C., Williams, R. J., Gozzard, E., & Newman, J. R. (2012). From existing in situ, high-resolution measurement technologies to lab-on-a-chip – the future of water quality monitoring?. Hydrology and earth system sciences discussions, 9(5), 6457-6506. https://doi.org/10.5194/hessd-9-6457-2012

2,6-Dibenzhydryl-N-(2-aryliminoacenaphthylenylidene)-4-chlorobenzenamino- palladium dichlorides: Synthesis, characterization, and use as catalysts in the Heck-reaction (2012)
Journal Article
Ban, Q., Zhang, J., Liang, T., Redshaw, C., & Sun, W. H. (2012). 2,6-Dibenzhydryl-N-(2-aryliminoacenaphthylenylidene)-4-chlorobenzenamino- palladium dichlorides: Synthesis, characterization, and use as catalysts in the Heck-reaction. Journal of organometallic chemistry, 713, 151-156. https://doi.org/10.1016/j.jorganchem.2012.05.015

A series of 2,6-dibenzhydryl-N-(2-aryliminoacenaphthylenylidene)-4- chlorobenzenaminopalladium(II) chloride complexes (C1-C6) were prepared and fully characterized by FT-IR and NMR spectroscopy, and by elemental analysis. The molecular structures of... Read More about 2,6-Dibenzhydryl-N-(2-aryliminoacenaphthylenylidene)-4-chlorobenzenamino- palladium dichlorides: Synthesis, characterization, and use as catalysts in the Heck-reaction.

Improved DNA extraction efficiency from low level cell numbers using a silica monolith based micro fluidic device (2012)
Journal Article
Kashkary, L., Kemp, C., Shaw, K. J., Greenway, G. M., & Haswell, S. J. (2012). Improved DNA extraction efficiency from low level cell numbers using a silica monolith based micro fluidic device. Analytica Chimica Acta, 750, 127-131. https://doi.org/10.1016/j.aca.2012.05.019

The evaluation of a micro fluidic system with an integrated silica monolith for performing DNA extraction from limited biological samples has been carried out. Low DNA target concentrations usually require the addition of carrier RNA to ensure desire... Read More about Improved DNA extraction efficiency from low level cell numbers using a silica monolith based micro fluidic device.

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